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Table 1 The total amount of 231Pa in the blank derived from the chemicals, including the spike, resin, Fe, and acids, and the total procedural blank, including filtering for an acid-cleaned 0.8 μm Pall Supor800 polyethersulfone filter (for small particulates) and 51 μm Sefar polyester mesh prefilter (for large particulates)

From: Improvements in the determination of attogram-sized 231Pa in dissolved and particulate fractions of seawater via multi-collector inductively coupled plasma mass spectrometry

Sample no.

231Pa

Error

Sample type

(ag/g)

/(2σ)

Chem-blank-1

0.015

0.008

Dissolved

Chem-blank-2

0.013

0.006

Dissolved

Chem-blank-3

0.025

0.008

Dissolved

Chem-blank-4

0.020

0.003

Dissolved

Chem-blank-5

0.025

0.004

Dissolved

Average

0.020

0.006

 

Sample no.

231Pa

Error

Sample type

(ag/g(1/8filter))

/(2σ)

GT8735db

65.559

0.011

Small particulate

GT8702db

8.212

0.003

Small particulate

GT9004db

25.652

0.007

Small particulate

GT9062db

29.761

0.006

Small particulate

GT9587db

50.132

0.006

Small particulate

GT9594db

34.950

0.005

Small particulate

GT9966db

85.845

0.012

Small particulate

GT9971db

38.720

0.006

Small particulate

GT8292db

11.115

0.001

Small particulate

GT8348db

62.386

0.004

Small particulate

GT3160db

16.289

0.008

Small particulate

GT3193db

9.858

0.004

Small particulate

GT2441db

16.165

0.004

Small particulate

GT2326db

9.326

0.006

Small particulate

GT2276db

41.427

0.009

Small particulate

Average

33.693

0.006

 

GT8824dbQP

21.450

0.009

Large particulate

GT8735dbQP

60.654

0.011

Large particulate

GT8702dbQP

26.372

0.008

Large particulate

GT9253dbQP

22.628

0.006

Large particulate

GT9971dbQP

27.383

0.009

Large particulate

GT3160dbQP

17.800

0.006

Large particulate

Average

29.381

0.008