E||a | E||b | E||c | Total | |||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Experiment | XH2O | H2O (ppm) | sd | n | H2O (ppm) | sd | n | H2O (ppm) | sd | n | H2O (ppm) | sd | Unpolarised H2O (ppm) | n |
[Si] integration range 3650–3420 cm−1 | ||||||||||||||
21 | 0.379 | 67 | 23 | 11 | 39 | 24 | 7 | 44 | 7 | 6 | 150 | 33 | 163 | 19 |
20 | 0.438 | 164 | 51 | 11 | 55 | 21 | 5 | 49 | 30 | 14 | 268 | 55 | 307 | 22 |
32 | 0.63 | 418 | 30 | 12 | 241 | 31 | 12 | 139 | 36 | 12 | 798 | 43 | 676 | 21 |
31 | 0.717 | 472 | 40 | 17 | 281 | 28 | 14 | 218 | 22 | 11 | 970 | 49 | 918 | 35 |
22 | 0.814 | 609 | 101 | 15 | 381 | 147 | 10 | 248 | 81 | 16 | 1239 | 178 | 1147 | 26 |
30 | 0.892 | 719 | 124 | 13 | 430 | 88 | 15 | 287 | 75 | 13 | 1436 | 152 | 1302 | 34 |
23 | 1 | 1208 | 104 | 10 | 661 | 138 | 8 | 444 | 43 | 7 | 2314 | 173 | 2087 | 14 |
[Mg] integration range 3268–3107 cm−1 | ||||||||||||||
84 | 0.56 | 16 | 4 | 11 | 16 | 4 | ||||||||
85 | 1 | 24 | 3 | 15 | 24 | 3 | ||||||||
[triv] integration range 3375–3293 cm−1 | ||||||||||||||
40 | 1 | 79 | 5 | 3 | 40 | 5 | 6 | 48 | 3 | 7 | 167 | 7 | ||
41 | 1 | 58 | 6 | 6 | 30 | 2 | 3 | 11 | 2 | 3 | 100 | 6 | ||
75 | 1 | 34 | 5 | 6 | 21 | 6 | 3 | 20 | 2 | 7 | 75 | 8 | ||
36 | 1 | 102 | 4 | 7 | 44 | 4 | 12 | 53 | 6 | 10 | 199 | 6 | 193 | 24 |
82 | 0.82 | 91 | 3 | 8 | 46 | 3 | 4 | 50 | 2 | 3 | 187 | 4 | 178 | 21 |
81 | 0.68 | 80 | 2 | 6 | 40 | 5 | 4 | 44 | 3 | 6 | 164 | 5 | 152 | 22 |
83 | 0.5 | 67 | 4 | 10 | 30 | 2 | 6 | 37 | 5 | 7 | 133 | 5 | 136 | 23 |
91 | 0.36 | 58 | 4 | 10 | 24 | 3 | 7 | 29 | 3 | 8 | 111 | 5 | 101 | 20 |
89 | 0.24 | 42 | 2 | 5 | 15 | 6 | 1 | 22 | 6 | 4 | 79 | 6 | 76 | 10 |
[Ti] integration range 3586–3495 cm−1 | ||||||||||||||
62 | 1 | 84 | 11 | 3 | 15 | 5 | 6 | 38 | 2 | 8 | 138 | 12 | 140 | 21 |
34 | 1 | 91 | 16 | 12 | 13 | 9 | 7 | 35 | 5 | 7 | 139 | 18 | 146 | 31 |
37 | 1 | 50 | 8 | 6 | 10 | 9 | 6 | 26 | 8 | 9 | 86 | 12 | 81 | 20 |
79 | 1 | 31 | 4 | 5 | 7 | 4 | 4 | 15 | 4 | 6 | 54 | 6 | 57 | 14 |
42 | 1 | 88 | 8 | 13 | 14 | 7 | 8 | 39 | 5 | 7 | 140 | 11 | 142 | 23 |
76 | 0.81 | 81 | 4 | 5 | 12 | 4 | 7 | 37 | 2 | 7 | 130 | 6 | 128 | 31 |
69 | 0.7 | 73 | 7 | 4 | 12 | 3 | 10 | 29 | 4 | 5 | 115 | 8 | 103 | 22 |
70 | 0.57 | 57 | 5 | 11 | 9 | 1 | 4 | 20 | 4 | 5 | 86 | 5 | 94 | 21 |
77 | 0.41 | 40 | 4 | 5 | 5 | 2 | 5 | 15 | 1 | 3 | 60 | 4 | 61 | 23 |
80 | 0.22 | 25 | 4 | 13 | 5 | 2 | 10 | 10 | 3 | 10 | 40 | 4 | 36 | 22 |